A library of C-alkyl and C-aryl nitrones has been obtained by direct condensation of primaryN-substituted hydroxylamine hydrochlorides with various aldehydes and ketones without catalystsor base. The synthetic procedure, performed under MW irradiation in the absence of solvent,does not require the presence of a base, is fast, clean, high-yielding and characterized by simplework-up.

Rapid, efficient and solvent free microwave mediated synthesis of aldo- and ketonitrones

Maiuolo L
;
De Nino A
;
2016-01-01

Abstract

A library of C-alkyl and C-aryl nitrones has been obtained by direct condensation of primaryN-substituted hydroxylamine hydrochlorides with various aldehydes and ketones without catalystsor base. The synthetic procedure, performed under MW irradiation in the absence of solvent,does not require the presence of a base, is fast, clean, high-yielding and characterized by simplework-up.
2016
1,3-Dipoles; Microwave; Neat reactions
File in questo prodotto:
Non ci sono file associati a questo prodotto.

I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.

Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/20.500.11770/132118
 Attenzione

Attenzione! I dati visualizzati non sono stati sottoposti a validazione da parte dell'ateneo

Citazioni
  • ???jsp.display-item.citation.pmc??? ND
  • Scopus 20
  • ???jsp.display-item.citation.isi??? 20
social impact